Extended knowledge of 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 30169-25-6, name is 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine, A new synthetic method of this compound is introduced below., name: 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine

Compound 1 (270 mg, 1.0 mmol) was placed in a 50 ml round bottomed flask. acetonitrile (10 ml) was added. 1,4 phenylene diamine (108 mg, 1.0 mmol) was added and the reaction heated to reflux for 1 hour. The reaction was allowed to cool to ambient temperature and the precipitate was isolated by filtration. The product was washed with cold acetonitrile, and air dried to give 225 mg of a purple solid (80% yield).

The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.