New learning discoveries about 1H-Pyrazole-4-carbonitrile

According to the analysis of related databases, 31108-57-3, the application of this compound in the production field has become more and more popular.

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 31108-57-3, name is 1H-Pyrazole-4-carbonitrile, This compound has unique chemical properties. The synthetic route is as follows., Safety of 1H-Pyrazole-4-carbonitrile

To a solution of crude reactant SC-II (100 mg, 0.241 mmol) in anhydrous THF (5 mL) was added lH-pyrazole-4-carbonitrile (112 mg, 1.2 mmol) followed by potassium carbonate (170 mg, 1.2 mmol) and the solution was heated at 60 C for 2h. Then the reaction mixture was diluted with ethyl acetate (100 mL). The resulting solution was washed with brine (2×50 mL), dried over magnesium sulfate and concentrated in vacuo. The crude product was purified by reverse phase prep-HPLC to afford product SB-21 (46 mg, 0.109 mmol, Yield=45%) as a white solid. 1HNMR (500 MHz, CDC13) 5(ppm): 7.86 (IH, s), 7.81 (IH, s), 5.00 (IH, AB), 4.92 (IH, AB), 2.61 (IH, t), 0.67 (3H, s), 0.67-2.25 (24H, m). LCMS: rt=2.47 mm, /z=424.2 [M+H]+

According to the analysis of related databases, 31108-57-3, the application of this compound in the production field has become more and more popular.