13599-12-7, name is Ethyl 3-phenyl-1H-pyrazole-5-carboxylate, belongs to pyrazoles-derivatives compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. COA of Formula: C12H12N2O2
General procedure: Pyrazole 1a-c (0.012 mol), the corresponding o-chloronitrobenzene 2a-c (0.012 mol) and powdered K2CO3 (0.50 mg, 0.036 mol) were successively mixed in DMF (3 ml). The reaction mixture was stirred at 50-80C for 3-6 h (TLC monitoring).The mixture was cooled, and water (5 ml) was added with stirring. The precipitate that formed was filtered off and recrystallized from ethanol.
The synthetic route of 13599-12-7 has been constantly updated, and we look forward to future research findings.