In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 113100-53-1 as follows. 113100-53-1
1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxylicacid 3 (7.50 mmol) and SOCl2 (30 mmol) were refluxed for 4 h. After the reaction is completed, the excess of SOCl2 was evaporated to give 4 as a yellow liquid that was used without further purification.
According to the analysis of related databases, 113100-53-1, the application of this compound in the production field has become more and more popular.