In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 930-36-9, name is 1-Methylpyrazole belongs to pyrazoles-derivatives compound, it is a common compound, a new synthetic route is introduced below. Recommanded Product: 930-36-9
A mixture of 1-methyl-1H-pyrazole (7) (37 gm, 0.6090 moles), iodine (57.1 gm,0.225 moles), hydrogen peroxide (9.2 gm, 0.27 moles) and DI water (I 10 ml) were stirred for 24 hour at 20-30C. Progress of the reaction was monitored by HPLC. The reaction mixture was cooled to 5-10C. The reaction mixture was quenched with 20% aqueous sodium bisulfate (100 ml) and stirred for I hour at 5-10C. The solid obtained was filtered,V washed with cold DI water (100 ml) and dried at 40-45C to obtain the product, 4-iodo-1-methyl- 1H-pyrazole. VDrywt : 56gmYield : 1.51 w/w(60%) V
The synthetic route of 930-36-9 has been constantly updated, and we look forward to future research findings.