Adding a certain compound to certain chemical reactions, such as: 30169-25-6, name is 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine, belongs to pyrazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 30169-25-6, Formula: C12H14N8
1,2,4,5-tetrazine-3,6-diamine (56 mg, 0.5 mmol) was added to 3,6-bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine (270 mg, 1 mmol) and K2CO3 (138 mg, 1 mmol) with 10 mL acetonitrile, and refluxed (80C) for 20 hours. Reaction was monitored with TLC using a 3:1 CCl4:CH3CN solvent system. The resulting dark, viscous solution was cooled with 10 mL ice water followed by 5% HCl added dropwise until the pH was about 1. The red precipitate was filtered and washed with water to yield 250 mg (109% yield, due to water in the sample).
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