Related Products of 75415-03-1,Some common heterocyclic compound, 75415-03-1, name is 2-(1H-Pyrazol-3-yl)pyridine, molecular formula is C8H7N3, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
A mixture of CuCl2¡¤4H2O (20.84 mg, 0.1 mmol), Hpzpy(28.84 mg, 0.2 mmol), DMF (3 mL) and H2O(1 mL) wassealed in a 25-ml Teflon-lined stainless container and heatedat 130 C for 72 h. After cooling to room temperature at arate of 5 C/h, colorless block crystals were obtained in ca.62% yield based on Cu. Anal. Calcd. for C18H18Cu2N6O6:C 39.93%, H 3.35%, N 15.52%; found C 39.84%, H 3.24%,N 15.48%. IR (KBr, cm-1): 3138 w, 2040 s, 1584 s, 1512 w,1438 m, 1372 w, 1245 w, 1089 s, 1028 w, 777 m, 723 m,705 w, 692 w, 623 m.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route 2-(1H-Pyrazol-3-yl)pyridine, its application will become more common.