{"id":6398,"date":"2021-09-18T05:53:13","date_gmt":"2021-09-17T21:53:13","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=6398"},"modified":"2021-09-18T05:53:13","modified_gmt":"2021-09-17T21:53:13","slug":"18-sep-news-sources-of-common-compounds-6825-71-4","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=6398","title":{"rendered":"18-Sep News Sources of common compounds: 6825-71-4"},"content":{"rendered":"

In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 6825-71-4 as follows. HPLC of Formula: C6H10N4O2<\/a><\/p>\n

To a solution of ethyl 3,5-diamino-1 -hydro-pyrazole-4-carboxylate (5.00 g, 29.38 mmol)In N, N-dimethylformamide ((80 mL)1,1,3,3-tetramethoxypropane (14.50 mL, 88.15 mmol)And acetic acid (0.34 mL, 5.88 mmol).After the reaction mixture was stirred at 100 C for 14 hours,Concentrate under reduced pressure. The resulting residue was dispersed in a mixed system of dichloromethane (50 mL) and water (50 mL), the organic phase was separated and the aqueous phase was extracted with dichloromethane (100 mL x 3). The combined organic phases were washed with saturated brine (100 mL x 3), dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The residue was purified by silica gel column chromatography (NH3 in methanol (7M) \/ methylene chloride (v \/ v) = 1\/100) to give the title compound as a pale yellow solid (3.52 g, 58.1%).<\/p>\n

According to the analysis of related databases, 6825-71-4, the application of this compound in the production field has become more and more popular.<\/p>\n

Reference:
Patent; Guangdong Dongyangguang Pharmaceutical Co., Ltd.; Jiatuo Sciences Corporation; Xi Ning; (88 pag.)CN104650092; (2017); B;<\/a>,
Pyrazole – Wikipedia<\/a>,
Pyrazoles – an overview | ScienceDirect Topics<\/p>\n","protected":false},"excerpt":{"rendered":"

According to the analysis of related databases, 6825-71-4, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[327,131],"tags":[126],"class_list":["post-6398","post","type-post","status-publish","format-standard","hentry","category-6825-71-4","category-pyrazoles-derivatives","tag-m-w100-200"],"yoast_head":"\nSources of common compounds:<\/title>\n<meta name=\"description\" content=\"In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 6825-71-4 as follows. 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