{"id":6259,"date":"2021-09-09T03:14:58","date_gmt":"2021-09-08T19:14:58","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=6259"},"modified":"2021-09-09T03:14:58","modified_gmt":"2021-09-08T19:14:58","slug":"september-92021-news-continuously-updated-synthesis-method-about-26308-42-9","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=6259","title":{"rendered":"September 9,2021 News Continuously updated synthesis method about 26308-42-9"},"content":{"rendered":"<p>In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 26308-42-9 as follows. <a href=\"https:\/\/www.ambeed.com\/products\/26308-42-9.html\">SDS of cas: 26308-42-9<\/a><\/p>\n<p>3-ethyl-1-methylpyrazole-5-carboxylic acid (10 mmol) thionyl chloride (25 mmol) and 1,2-dichloroethane (15 mL) were reacted under reflux and stirring for 3-4 hours.After cooling, the solvent and excess thionyl chloride were removed under reduced pressure to give the title compound 1. 3 g.<\/p>\n<p>According to the analysis of related databases, 26308-42-9, the application of this compound in the production field has become more and more popular.<\/p>\n<p>Reference:<br \/><a href=\"https:\/\/doi.org\/10.1021\/jf204778v\">Patent; Huang, Danling; Hunan Research Institute of Chemical Industry ltd; Liu, Aiping; Huang, Mingzhi; Li, Jianming; Wang, xiaoguang; Liu, Weidong; Chen, Xiao Yang; He, Lian; Xiang, Jun; Pei, Hui; (24 pag.)CN106608873; (2017); A;<\/a>,<br \/><a href=\"https:\/\/en.wikipedia.org\/wiki\/Pyrazole\">Pyrazole &#8211; Wikipedia<\/a>,<br \/><a href=\"https:\/\/www.sciencedirect.com\/topics\/chemistry\/pyrazoles\">Pyrazoles &#8211; an overview | ScienceDirect Topics<\/p>\n","protected":false},"excerpt":{"rendered":"<p>According to the analysis of related databases, 26308-42-9, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[130,131],"tags":[126],"class_list":["post-6259","post","type-post","status-publish","format-standard","hentry","category-26308-42-9","category-pyrazoles-derivatives","tag-m-w100-200"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.9 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Continuously updated synthesis method about<\/title>\n<meta name=\"description\" content=\"In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. 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