{"id":4718,"date":"2021-06-15T04:36:48","date_gmt":"2021-06-14T20:36:48","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=4718"},"modified":"2021-06-15T04:36:48","modified_gmt":"2021-06-14T20:36:48","slug":"share-a-compound-3-methylpyrazole-3","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=4718","title":{"rendered":"Share a compound : 3-Methylpyrazole"},"content":{"rendered":"

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1453-58-3, name is 3-Methylpyrazole, This compound has unique chemical properties. The synthetic route is as follows., Application In Synthesis of 3-Methylpyrazole<\/a><\/p>\n

250 mL of dimethyl sulfoxide and sodium hydride 24.0 g (60percent, petroleum ether washing) were added to a three-necked flask, and 41.0 g of 3-methylpyrazole was dissolved in 150 mL of dimethyl sulfoxide, and slowly added to the reaction flask. The reaction was carried out until no bubbles were evolved, and 101.5 g of p-methoxybenzyl bromide was added to maintain the temperature of the reaction system at 30 \u00b0C. After the reaction was completed, 1 L of ice water was added, and dichloromethane (200 mL \u00d7 3) was added, and the organic phase was combined, washed with water, washed with saturated sodium hydrogen carbonate, brine, and dried over anhydrous sodium sulfate.Concentration gave 99.6 g (98.5percent) of 1-(4′-methoxybenzyl)-3-methylpyrazole.<\/p>\n

According to the analysis of related databases, 1453-58-3, the application of this compound in the production field has become more and more popular.<\/p>\n

Reference:
Patent; Nantong University; Tang Yanfeng; Ding Xinyu; Shan Jiahui; Yu Hongmei; Wang Shuqing; Mao Jiarong; Guo Xiaoqing; (5 pag.)CN103880749; (2019); B;<\/a>,
Pyrazole – Wikipedia<\/a>,
Pyrazoles – an overview | ScienceDirect Topics<\/p>\n","protected":false},"excerpt":{"rendered":"

According to the analysis of related databases, 1453-58-3, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[175,131],"tags":[145],"class_list":["post-4718","post","type-post","status-publish","format-standard","hentry","category-1453-58-3","category-pyrazoles-derivatives","tag-m-w0-100"],"yoast_head":"\nShare a compound :<\/title>\n<meta name=\"description\" content=\"Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1453-58-3, name is 3-Methylpyrazole, This compound has unique chemical properties. 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