{"id":1767,"date":"2021-02-18T05:48:17","date_gmt":"2021-02-17T21:48:17","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=1767"},"modified":"2021-02-18T05:48:17","modified_gmt":"2021-02-17T21:48:17","slug":"brief-introduction-of-30169-25-6","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=1767","title":{"rendered":"Brief introduction of 30169-25-6"},"content":{"rendered":"

Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 30169-25-6, name is 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine, A new synthetic method of this compound is introduced below., Quality Control of 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine<\/a><\/p>\n

Benzimidazole (248 mg, 2.1 mmol) was added to tetrazine 1a (270 mg, 1 mmol) in acetonitrile (5 mL), the mixture was stirred for 3 h with heating to 75 C. Then, after hot filtration, the substance was washed with hot acetonitrile on the filter. The yield was 299 mg (95%). A red powder, m.p. 332-334 C. Found (%): C, 60.74; H, 3.41; N, 35.42. C16H10N8. Calculated (%): C, 61.14; H, 3.21; N, 35.65. 1H NMR (DMSO-d6), delta: 7.48-7.55, 7.56-7.62, 7.91-7.97, 8.45-8.52 (both m, 2 H each, H(4), H(5), H(6), H(7) in benzimidazolyls); 9.43 (both s, 2 H each, H(2) in benzimidazolyls). 13C NMR (DMSO-d6), delta: it was technically impossible to register 13C NMR spectrum because of the poor solubility of compound 1d.<\/p>\n

The synthetic route of 30169-25-6 has been constantly updated, and we look forward to future research findings.<\/p>\n","protected":false},"excerpt":{"rendered":"

The synthetic route of 30169-25-6 has been constantly updated, and we look forward to future research findings.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[370,131],"tags":[127],"class_list":["post-1767","post","type-post","status-publish","format-standard","hentry","category-30169-25-6","category-pyrazoles-derivatives","tag-m-w200-300"],"yoast_head":"\nBrief introduction of 30169-25-6<\/title>\n<meta name=\"description\" content=\"Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. 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Pyrazole derivatives play an important role in antitumor agents.\",\"potentialAction\":[{\"@type\":\"SearchAction\",\"target\":{\"@type\":\"EntryPoint\",\"urlTemplate\":\"https:\/\/www.pyrazoles-derivatives.com\/?s={search_term_string}\"},\"query-input\":{\"@type\":\"PropertyValueSpecification\",\"valueRequired\":true,\"valueName\":\"search_term_string\"}}],\"inLanguage\":\"en-US\"},{\"@type\":\"Person\",\"@id\":\"https:\/\/www.pyrazoles-derivatives.com\/#\/schema\/person\/d9a9f27bed675392c6f363a01ffd49f1\",\"name\":\"Jessica.F\",\"image\":{\"@type\":\"ImageObject\",\"inLanguage\":\"en-US\",\"@id\":\"https:\/\/www.pyrazoles-derivatives.com\/#\/schema\/person\/image\/\",\"url\":\"https:\/\/en.cravatar.com\/avatar\/2d1cec2a99eeaad5a5b217c9cdbfb610?s=96&d=mm&r=g\",\"contentUrl\":\"https:\/\/en.cravatar.com\/avatar\/2d1cec2a99eeaad5a5b217c9cdbfb610?s=96&d=mm&r=g\",\"caption\":\"Jessica.F\"}}]}<\/script>\n<!-- \/ Yoast SEO plugin. -->","yoast_head_json":{"title":"Brief introduction of 30169-25-6","description":"Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. 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