{"id":1748,"date":"2021-02-10T05:17:53","date_gmt":"2021-02-09T21:17:53","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=1748"},"modified":"2021-02-10T05:17:53","modified_gmt":"2021-02-09T21:17:53","slug":"introduction-of-a-new-synthetic-route-about-52867-42-2","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=1748","title":{"rendered":"Introduction of a new synthetic route about 52867-42-2"},"content":{"rendered":"<p><a href=\"https:\/\/www.ambeed.com\/products\/52867-42-2.html\">Application of 52867-42-2<\/a>, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 52867-42-2 as follows.<\/p>\n<p>Reference Example 61 Production of methyl 3-(2-methoxyethoxy)-1-methyl-1H-pyrazole-5-carboxylate Using methyl 3-hydroxy-1-methyl-1H-pyrazole-5-carboxylate (2.34 g, 15.0 mmol), 1-bromo-2-methoxyethane (3.13 g, 22.5 mmol), potassium carbonate (4.15 g, 30.0 mmol) and N,N-dimethylformamide (15 mL), and in the same manner as in Reference Example 57, the title compound (3.03 g, yield 94%) was obtained. 1H-NMR (DMSO-d6, 300 MHz) delta 3.28 (3H, s), 3.57-3.64 (2H, m), 3.81 (3H, s), 3.93 (3H, s), 4.14-4.20 (2H, m), 6.28 (1H, s).<\/p>\n<p>According to the analysis of related databases, 52867-42-2, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>According to the analysis of related databases, 52867-42-2, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[237,131],"tags":[126],"class_list":["post-1748","post","type-post","status-publish","format-standard","hentry","category-52867-42-2","category-pyrazoles-derivatives","tag-m-w100-200"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.9 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Introduction of a new synthetic route about 52867-42-2<\/title>\n<meta name=\"description\" content=\"Application of 52867-42-2, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. 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