{"id":1742,"date":"2021-02-10T05:17:53","date_gmt":"2021-02-09T21:17:53","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=1742"},"modified":"2021-02-10T05:17:53","modified_gmt":"2021-02-09T21:17:53","slug":"analyzing-the-synthesis-route-of-6314-23-4","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=1742","title":{"rendered":"Analyzing the synthesis route of 6314-23-4"},"content":{"rendered":"<p>Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6314-23-4, name is 2-(1-Pyrazolyl)ethanol, This compound has unique chemical properties. The synthetic route is as follows., <a href=\"https:\/\/www.ambeed.com\/products\/6314-23-4.html\">name: 2-(1-Pyrazolyl)ethanol<\/a><\/p>\n<p>A mixture of 2- (LH-PYRAZOL-1-YL) ethanol (6.76 g) and potassium tert-butoxide (6.75 g) in tetrahydrofuran (100 ml) was stirred at ambient temperature for an hour. A solution of 1-fluoro-4-nitrobenzene (7.1 g) in tetrahydrofuran (5 ml) was added to the above mixture and refluxed under stirring for 2.5 hours. The reaction mixture was poured into a mixture of ethyl acetate and water, and the organic layer was washed with brine and dried over magnesium sulfate. The solvent was concentrated in vacuo and the precipitate was collected by filtration to give 1- [2- (4-NITROPHENOXY) ETHYL]-LH-PYRAZOLE (10.75 G). 1H-NMR (DMSO-d6): 8 4. 47-4.60 (4H, m), 6.27 (1H, m), 7.08-7. 16 (2H, m), 7.49 (1H, d, J=1.7 Hz), 7.81 (1H, d, J=2.0 Hz), 8.16- 8.23 (2H, m)<\/p>\n<p>According to the analysis of related databases, 6314-23-4, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>According to the analysis of related databases, 6314-23-4, the application of this compound in the production field has become more and more popular.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[365,131],"tags":[126],"class_list":["post-1742","post","type-post","status-publish","format-standard","hentry","category-6314-23-4","category-pyrazoles-derivatives","tag-m-w100-200"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.9 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Analyzing the synthesis route of 6314-23-4<\/title>\n<meta name=\"description\" content=\"Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6314-23-4, name is 2-(1-Pyrazolyl)ethanol, This compound has unique chemical properties. 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