{"id":1407,"date":"2021-01-08T10:46:10","date_gmt":"2021-01-08T02:46:10","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=1407"},"modified":"2021-01-08T10:46:10","modified_gmt":"2021-01-08T02:46:10","slug":"new-downstream-synthetic-route-of-3112-31-0","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=1407","title":{"rendered":"New downstream synthetic route of 3112-31-0"},"content":{"rendered":"

Reference of 3112-31-0<\/a>, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3112-31-0, name is 1H-Pyrazole-3,5-dicarboxylic acid, This compound has unique chemical properties. The synthetic route is as follows.<\/p>\n

The deionized water (3 mL) was slowly dropped over the mixturesolution containing Cu(NO3)23H2O (0.2 mmol, 48 mg) andpyrazine (0.2 mmol, 16 mg) in water and DMF (4 mL, 1:1 v\/v) in15 mL of glass vial. Then, the solution of pyrazole-3,5-dicarboxylicacid (0.2 mmol, 35 mg) in deionized water and ethanol (5 mL,1:1 v\/v) was carefully layered over the mixture layer. Then, the vialwas sealed and allowed to stand undisturbed at room temperature. The blue crystals of 1 were obtained after 2 days. Yield: 16 mg(34percent) based on copper salt. Anal. Calcd for Cu3C14H20N6O15: C,23.92; H, 2.87; N, 11.95. Found: C, 24.40; H, 2.80; N, 11.73percent. FTIRpeaks (KBr, cm-1): 3367br (m(OH)), 1622s (mas(OCO)), 1609s (m(CN)), 1509m, 1423w, 1395m (ms(OCO)), 1341s, 1330s, 1297s,1157w, 1127w, 1100w, 1063w, 1028w, 1017w, 930w, 828w,797w. UV-vis (diffuse reflectance, cm-1): 14049.<\/p>\n

The chemical industry reduces the impact on the environment during synthesis 1H-Pyrazole-3,5-dicarboxylic acid. I believe this compound will play a more active role in future production and life.<\/p>\n","protected":false},"excerpt":{"rendered":"

The chemical industry reduces the impact on the environment during synthesis 1H-Pyrazole-3,5-dicarboxylic acid. I believe this compound will play a more active role in future production and life.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[140,131],"tags":[126],"class_list":["post-1407","post","type-post","status-publish","format-standard","hentry","category-3112-31-0","category-pyrazoles-derivatives","tag-m-w100-200"],"yoast_head":"\nNew downstream synthetic route of 3112-31-0<\/title>\n<meta name=\"description\" content=\"Reference of 3112-31-0, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3112-31-0, name is 1H-Pyrazole-3,5-dicarboxylic acid, This compound has unique chemical properties. The synthetic route is as follows.\" \/>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" href=\"https:\/\/www.pyrazoles-derivatives.com\/?p=1407\" \/>\n<meta property=\"og:locale\" content=\"en_US\" \/>\n<meta property=\"og:type\" content=\"article\" \/>\n<meta property=\"og:title\" content=\"New downstream synthetic route of 3112-31-0\" \/>\n<meta property=\"og:description\" content=\"Reference of 3112-31-0, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 3112-31-0, name is 1H-Pyrazole-3,5-dicarboxylic acid, This compound has unique chemical properties. 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