{"id":1387,"date":"2021-01-06T10:56:35","date_gmt":"2021-01-06T02:56:35","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=1387"},"modified":"2021-01-06T10:56:35","modified_gmt":"2021-01-06T02:56:35","slug":"simple-exploration-of-13599-12-7","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=1387","title":{"rendered":"Simple exploration of 13599-12-7"},"content":{"rendered":"

13599-12-7, name is Ethyl 3-phenyl-1H-pyrazole-5-carboxylate, belongs to pyrazoles-derivatives compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. COA of Formula: C12H12N2O2<\/a><\/p>\n

General procedure: Pyrazole 1a-c (0.012 mol), the corresponding o-chloronitrobenzene 2a-c (0.012 mol) and powdered K2CO3 (0.50 mg, 0.036 mol) were successively mixed in DMF (3 ml). The reaction mixture was stirred at 50-80C for 3-6 h (TLC monitoring).The mixture was cooled, and water (5 ml) was added with stirring. The precipitate that formed was filtered off and recrystallized from ethanol.<\/p>\n

The synthetic route of 13599-12-7 has been constantly updated, and we look forward to future research findings.<\/p>\n","protected":false},"excerpt":{"rendered":"

The synthetic route of 13599-12-7 has been constantly updated, and we look forward to future research findings.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[282,131],"tags":[127],"class_list":["post-1387","post","type-post","status-publish","format-standard","hentry","category-13599-12-7","category-pyrazoles-derivatives","tag-m-w200-300"],"yoast_head":"\nSimple exploration of 13599-12-7<\/title>\n<meta name=\"description\" content=\"13599-12-7, name is Ethyl 3-phenyl-1H-pyrazole-5-carboxylate, belongs to pyrazoles-derivatives compound, is considered to be a conventional heterocyclic compound, which is widely used in drug synthesis. The chemical synthesis route is as follows. 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