{"id":1371,"date":"2021-01-05T16:52:55","date_gmt":"2021-01-05T08:52:55","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=1371"},"modified":"2021-01-05T16:52:55","modified_gmt":"2021-01-05T08:52:55","slug":"extracurricular-laboratory-synthetic-route-of-83725-05-7-2","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=1371","title":{"rendered":"Extracurricular laboratory: Synthetic route of 83725-05-7"},"content":{"rendered":"<p>Adding a certain compound to certain chemical reactions, such as: 83725-05-7, name is N-(5-Methyl-1H-pyrazol-3-yl)acetamide, belongs to pyrazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound  83725-05-7, <a href=\"https:\/\/www.ambeed.com\/products\/83725-05-7.html\">HPLC of Formula: C6H9N3O<\/a><\/p>\n<p>4.1.2 N-(5-methyl-4-nitro-1H-pyrazol-3-yl)acetamide (3) Compound 2 (4.5g, 32?mmol) was dissolved in 50?mL concentrated H2SO4, and the solution was cooled to -5?C. Concentrated HNO3 (2.3?mL, 32?mmol) was added dropwise and the mixture was maintained at -5?C for 3?h. The reaction mixture was added to 150?mL ice water slowly, and then white solid appeared with stirring. The solid washed by water and dried to give pure 3 (4.65?g, 25?mmol, 72% yield). Mp: 240-241?C; 1H NMR (400?MHz, DMSO-d6) delta 10.24 (s, 1H), 2.45 (s, 3H), 2.13 (s, 3H).<\/p>\n<p>In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, N-(5-Methyl-1H-pyrazol-3-yl)acetamide, other downstream synthetic routes, hurry up and to see.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, N-(5-Methyl-1H-pyrazol-3-yl)acetamide, other downstream synthetic routes, hurry up and to see.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[277,131],"tags":[126],"class_list":["post-1371","post","type-post","status-publish","format-standard","hentry","category-83725-05-7","category-pyrazoles-derivatives","tag-m-w100-200"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.9 - https:\/\/yoast.com\/wordpress\/plugins\/seo\/ -->\n<title>Extracurricular laboratory: Synthetic route of 83725-05-7<\/title>\n<meta name=\"description\" content=\"Adding a certain compound to certain chemical reactions, such as: 83725-05-7, name is N-(5-Methyl-1H-pyrazol-3-yl)acetamide, belongs to pyrazoles-derivatives compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. 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