{"id":11822,"date":"2022-12-05T06:01:02","date_gmt":"2022-12-04T22:01:02","guid":{"rendered":"https:\/\/www.pyrazoles-derivatives.com\/?p=11822"},"modified":"2022-12-05T06:01:02","modified_gmt":"2022-12-04T22:01:02","slug":"idemudia-omoruyi-g-s-team-published-research-in-zeitschrift-fuer-kristallographie-new-crystal-structures-in-229-cas-4551-69-3","status":"publish","type":"post","link":"https:\/\/www.pyrazoles-derivatives.com\/?p=11822","title":{"rendered":"Idemudia, Omoruyi G.&#8217;s team published research in Zeitschrift fuer Kristallographie &#8211; New Crystal Structures  in 229 | CAS: 4551-69-3"},"content":{"rendered":"<p>Idemudia, Omoruyi G. published the artcile<b><i>Crystal structure of 4-benzoyl-3-methyl-1-phenyl-2-pyrazolin-5-one sulfadiazine dimethylformamide monosolvate, C<sub>30<\/sub>H<sub>29<\/sub>N<sub>7<\/sub>O<sub>4<\/sub>S<\/i><\/b>,  <a href=\"https:\/\/www.ambeed.com\/products\/4551-69-3.html\">Name:  4-Benzoyl-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one<\/a>,  the publication is  Zeitschrift fuer Kristallographie &#8211; New Crystal Structures (2014), 229(4), 455-457, database is CAplus.<\/p>\n<p>The crystal and mol. structure of a 4-benzoyl-3-methyl-1-phenyl-2-pyrazolin-5-one Schiff base with sulfadiazine is presented. In the asym. unit the title compound occurs together with 1 DMF solvent mol. There are 2 notable intramol. H bonds, both with O1, namely N3-H3\u00b7\u00b7\u00b7O1 and C12-H12\u00b7\u00b7\u00b7O1 that hold the phenylpyrazolone backbone essentially planar together with extended resonance. The least square plane through the atoms N1-N3, O1, C1-C3, C5, and C11-C16 has a r.m.s. of 0.0671 \u00c5. Adjacent mols. are held together at the sulfadiazine group with 2 short N4-H4\u00b7\u00b7\u00b7N6 H bonds with lengths of 2.062(19) \u00c5 which in terms of graph-set anal. can be described by means of a R<sup>2<\/sup><sub>2<\/sub>(8) descriptor on the unary level. There are a large number of \u03c0\u00b7\u00b7\u00b7\u03c0 ring interactions. The 2 shortest interactions occur with the Ph ring C31-C36 which has 2 \u03c0\u00b7\u00b7\u00b7\u03c0 ring interactions; 1 with an adjacent pyrazole ring N1, N2, C1-C3, and 1 with the Ph ring C11-C16. The centroid to centroid distances are 4.2512(8) and 4.2530(9) \u00c5, resp. The crystal contains the solvent DMF positionally disordered in a 0.82:0.18 ratio. Crystallog. data are given.<\/p>\n<p>Zeitschrift fuer Kristallographie &#8211; New Crystal Structures published new progress about 4551-69-3. 4551-69-3 belongs to pyrazoles-derivatives, auxiliary class Benzenes, name is 4-Benzoyl-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one, and the molecular formula is C17H14N2O2, <a href=\"https:\/\/www.ambeed.com\/products\/4551-69-3.html\">Name:  4-Benzoyl-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one<\/a>.<\/p>\n<p>Referemce:<br \/><a href=\"https:\/\/en.wikipedia.org\/wiki\/Pyrazole\">https:\/\/en.wikipedia.org\/wiki\/Pyrazole<\/a>,<br \/><a href=\"Pyrazole - Wikipedia\">Pyrazoles &#8211; an overview | ScienceDirect Topics<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>Zeitschrift fuer Kristallographie &#8211; New Crystal Structures published new progress about 4551-69-3. 4551-69-3 belongs to pyrazoles-derivatives, auxiliary class Benzenes, name is 4-Benzoyl-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one, and the molecular formula is C17H14N2O2, <a href=\"https:\/\/www.ambeed.com\/products\/4551-69-3.html\">Name:  4-Benzoyl-5-methyl-2-phenyl-2,4-dihydro-3H-pyrazol-3-one<\/a>.<\/p>\n","protected":false},"author":8,"featured_media":0,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[808,131],"tags":[740],"class_list":["post-11822","post","type-post","status-publish","format-standard","hentry","category-4551-69-3","category-pyrazoles-derivatives","tag-m-w250-300"],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v24.9 - 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